Methyl (2-{[(tert-butoxycarbonyl)amino]methyl}phenyl)acetate → HCID 14180954, compound

HRID 1612406Notes

Reaction equation

HRID 1612406 reaction equation
C[O:2][C:3](=[O:17])[CH2:4][C:5]1[CH:10]=[CH:9][C:8]([CH2:11][NH:12][S:13]([CH3:16])(=[O:15])=[O:14])=[CH:7][CH:6]=1.COC(=O)CC1C=CC=CC=1CNC(OC(C)(C)C)=O>>[CH3:16][S:13]([NH:12][CH2:11][C:8]1[CH:9]=[CH:10][C:5]([CH2:4][C:3]([OH:17])=[O:2])=[CH:6][CH:7]=1)(=[O:15])=[O:14]

Participants

3

Reactant 2

HCID 53438887Methyl (2-{[(tert-butoxycarbonyl)amino]methyl}phenyl)acetateHCID 69587389HCID 69587389, compound

Product 1

HCID 14180954HCID 14180954, compound

Procedure

Compound 12a was prepared by following the procedure of Example 1, Step e, except 11a was substituted for 5a. (54%) Mass Spectral Analysis m/z=242.2 (M−H)− tR=1.47 min (96%)

Sources & evidence

ORD record
ord-0e2583e92851457da1d56e36bd720c8f
Source dataset
uspto-grants-2006_01
Patent number
US06992193B2

Reaction notes

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