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HRID1612447

反应详情

EQUATION

反应方程式

HRID 1612447 的结构方程式

REACTANTS

反应物

2
结构：CC(C)=CCBr
HCID70092

2-Butene, 1-bromo-3-methyl-

C5H9Br

结构：CC1CC([C@H](Cc2ccccc2)NC(=O)OC(C)(C)C)OC1=O
HCID57181317

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)=CC[C@@H]1C[C@@H]([C@H](Cc2ccccc2)NC(=O)OC(C)(C)C)OC1=O
HCID12015737

未命名化合物

收率 84%

PROCEDURE

实验过程

Prepared analogously to the synthesis of [(S)-1-(4-Methyl-5-oxo-tetrahydrofuran-2-yl)-2-phenylethyl]carbamic acid t-butyl ester in Journal of Organic Chemistry (1986) 51(21), 3921, using 4-bromo-2-methyl-2-butene in place of methyl iodide, to afford D30 in 84% yield.

WORKUP

后处理

  1. customto afford D30 in 84% yield