HRID1612448

反应详情

EQUATION

反应方程式

HRID 1612448 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

[(1S,2S,4R)-1-Benzyl-4-(bicyclo[2.2.1]hept-2-ylcarbamoyl)-2-hydroxy-7-methyl-oct-6-enyl]carbamic acid tert-butyl ester (D31) (1.61 g, 3.33 mmol) in methanol (30 ml) was hydrogenated over 10% Pd/C (300 mg) for 3.75 h. The catalyst was filtered and the filtrate evaporated to afford D32 1.51 g.

WORKUP

后处理

  1. filtrationThe catalyst was filtered
  2. customthe filtrate evaporated
  3. customto afford D32 1.51 g