HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,8-Diazabicyclo(5.4.0)undec-7-ene → Dimethyl 5-(2-oxopyrrolidin-1-yl)isophthalate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | 5-(4-Bromo-butanoylamino)-isophthalic Acid Dimethyl Ester | HCID 69589718 | — |
| Product | Dimethyl 5-(2-oxopyrrolidin-1-yl)isophthalate | HCID 57513093 | 35% |
Reaction Steps
5-(4-Bromo-butanoylamino)-isophthalic acid dimethyl ester (D61) was treated with DBU as described in D57 to afford D62 as a white solid (35%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06992103B2 |
| Source dataset | uspto-grants-2006_01 |
| ORD ID | ord-f8ccfd99d66a47a7986c84bde8e1acb8 |
| Source note | uspto-grants-2006_01 |