HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl-2-thienylmethyl chloride → 4-(phenyl-2-thienylmethoxy)-1-[4-(2-nitrophenoxy)-2(Z)-butenyl]piperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl-2-thienylmethyl chloride | HCID 10512583 | — |
| Reactant | 4-hydroxy-1-[4-(2-nitrophenoxy)-2(E)-butenyl]piperidine | HCID 19776719 | — |
| Reactant | 4-hydroxy-1-[4-(2-nitrophenoxy)-2(Z)-butenyl]piperidine | HCID 67878343 | — |
| Product | 4-(phenyl-2-thienylmethoxy)-1-[4-(2-nitrophenoxy)-2(Z)-butenyl]piperidine | HCID 67879049 | — |
Reaction Steps
The procedure of Example 39 (a) was repeated except for using phenyl-2-thienylmethyl chloride and 4-hydroxy-1-[4-(2-nitrophenoxy)-2(Z)-butenyl]piperidine instead of phenyl-2-thienylmethyl chloride and 4-hydroxy-1-[4-(2-nitrophenoxy)-2(E)-butenyl]piperidine to give oily 4-(phenyl-2-thienylmethoxy)-1-[4-(2-nitrophenoxy)-2(Z)-butenyl]piperidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05190959 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-c834ac93cae64bdd91555054e46d329c |
| Source note | uspto-grants-1993_03 |