Sodium Carbonate → HCID 19776698, compound

HRID 1612851Notes

Reaction equation

HRID 1612851 reaction equation
Cl.[C:2]1([CH:8]([C:29]2[CH:33]=[CH:32][S:31][CH:30]=2)[O:9][CH:10]2[CH2:15][CH2:14][N:13]([CH2:16][CH2:17][CH2:18][O:19][C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][C:21]=3[N+:26]([O-:28])=[O:27])[CH2:12][CH2:11]2)[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C(=O)([O-])[O-].[Na+].[Na+]>>[C:2]1([CH:8]([C:29]2[CH:33]=[CH:32][S:31][CH:30]=2)[O:9][CH:10]2[CH2:11][CH2:12][N:13]([CH2:16][CH2:17][CH2:18][O:19][C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][C:21]=3[N+:26]([O-:28])=[O:27])[CH2:14][CH2:15]2)[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 10340Sodium CarbonateHCID 19776759HCID 19776759, compound

Product 1

HCID 19776698HCID 19776698, compound

Procedure

The hydrochloride obtained in the above was treated with 5% aqueous sodium carbonate in the same way as in Example 36 (a) to give oily 4-(phenyl-3-thienylmethoxy)-1-[3-(2-nitrophenoxy)propyl]piperidine.

Sources & evidence

ORD record
ord-15c3432a276d45b1ad0c3e54d33239e3
Source dataset
uspto-grants-1993_03
Patent number
US05190959

Reaction notes

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