HCID 19776762, compound → HCID 19776706, compound

HRID 1612852Notes

Reaction equation

HRID 1612852 reaction equation
[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6](Cl)[C:7]1[S:8][CH:9]=[CH:10][CH:11]=1.[OH:13][CH:14]1[CH2:19][CH2:18][N:17]([CH2:20][CH2:21][CH2:22][O:23][C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][C:25]=2[N+:30]([O-:32])=[O:31])[CH2:16][CH2:15]1>>[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]([C:7]1[S:8][CH:9]=[CH:10][CH:11]=1)[O:13][CH:14]1[CH2:15][CH2:16][N:17]([CH2:20][CH2:21][CH2:22][O:23][C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][C:25]=2[N+:30]([O-:32])=[O:31])[CH2:18][CH2:19]1

Participants

3

Reactant 2

HCID 19776762HCID 19776762, compoundHCID 197767934-Hydroxy-1-[3-(2-nitrophenoxy)propyl]piperidine2×

Product 1

HCID 19776706HCID 19776706, compound

Procedure

The procedure of Example 36 (a) was repeated except for using di(2-thienyl)methyl chloride and 4-hydroxy-1-[3-(2-nitrophenoxy)propyl]piperidine instead of phenyl-2-thienylmethyl chloride and 4-hydroxy-1-[3-(2-nitrophenoxy)propyl]piperidine to give oily 4-di(2-thienyl)methoxy-1-[3-(2-nitrophenoxy)propyl]piperidine.

Sources & evidence

ORD record
ord-d70b495b24ad4ba29d246318cee764ff
Source dataset
uspto-grants-1993_03
Patent number
US05190959

Reaction notes

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