Sodium Carbonate → HCID 19776771, compound

HRID 1612853Notes

Reaction equation

HRID 1612853 reaction equation
Cl.[S:2]1[CH:6]=[CH:5][CH:4]=[C:3]1[CH:7]([C:28]1[CH:32]=[CH:31][S:30][CH:29]=1)[O:8][CH:9]1[CH2:14][CH2:13][N:12]([CH2:15][CH2:16][CH2:17][O:18][C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][C:20]=2[N+:25]([O-:27])=[O:26])[CH2:11][CH2:10]1.C(=O)([O-])[O-].[Na+].[Na+]>>[S:2]1[CH:6]=[CH:5][CH:4]=[C:3]1[CH:7]([C:28]1[CH:32]=[CH:31][S:30][CH:29]=1)[O:8][CH:9]1[CH2:10][CH2:11][N:12]([CH2:15][CH2:16][CH2:17][O:18][C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][C:20]=2[N+:25]([O-:27])=[O:26])[CH2:13][CH2:14]1

Participants

3

Reactant 2

HCID 10340Sodium CarbonateHCID 19776826HCID 19776826, compound

Product 1

HCID 19776771HCID 19776771, compound

Procedure

The hydrochloride obtained in the above was treated with 5% aqueous sodium carbonate to give oily 4-[(2-thienyl)-3-thienylmethoxy]-1-[3-(2-nitrophenoxy)propyl]piperidine.

Sources & evidence

ORD record
ord-70a7b143575346ffb39e1d5bf6745ddf
Source dataset
uspto-grants-1993_03
Patent number
US05190959

Reaction notes

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