1-(3-Chloro-propoxy)-2-nitro-benzene → HCID 19776756, compound

HRID 1612859Notes

Reaction equation

HRID 1612859 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([CH:7]([C:15]2[S:16][CH:17]=[CH:18][CH:19]=2)[O:8][CH:9]2[CH2:14][CH2:13][NH:12][CH2:11][CH2:10]2)[CH:2]=1.Cl[CH2:21][CH2:22][CH2:23][O:24][C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][C:26]=1[N+:31]([O-:33])=[O:32]>>[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([CH:7]([C:15]2[S:16][CH:17]=[CH:18][CH:19]=2)[O:8][CH:9]2[CH2:14][CH2:13][N:12]([CH2:21][CH2:22][CH2:23][O:24][C:25]3[CH:30]=[CH:29][CH:28]=[CH:27][C:26]=3[N+:31]([O-:33])=[O:32])[CH2:11][CH2:10]2)[CH:2]=1

Participants

3

Reactant 2

HCID 114244631-(3-Chloro-propoxy)-2-nitro-benzene2×HCID 19776797HCID 19776797, compound

Product 1

HCID 19776756HCID 19776756, compound

Procedure

The procedure of Example 24 (a) was repeated except for using 4-[(3-pyridyl)-2-thienylmethoxy]piperidine and 1-chloro-3-(2-nitrophenoxy)propane instead of 4-[(2-chlorophenyl)-phenylmethoxy]piperidine and 1-chloro-3-(2-nitrophenoxy)propane to give oily 4-[(3-pyridyl)-2-thienylmethoxy]-1-[3-(2-nitrophenoxy)propyl]piperidine.

Sources & evidence

ORD record
ord-d634770d21044506af32815a8761eb9a
Source dataset
uspto-grants-1993_03
Patent number
US05190959

Reaction notes

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