HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxy-1-[3-(4-methyl-2-nitrophenoxy)propyl]piperidine → 4-Di(3-thienyl)methoxy-1-[3-(4-methyl-2-nitrophenoxy)propyl]piperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxy-1-[3-(4-methyl-2-nitrophenoxy)propyl]piperidine | HCID 19776693 | — |
| Reactant | Di(3-thienyl)methyl chloride | HCID 19776723 | — |
| Reactant | 4-Hydroxy-1-[3-(2-nitrophenoxy)propyl]piperidine | HCID 19776793 | — |
| Product | 4-Di(3-thienyl)methoxy-1-[3-(4-methyl-2-nitrophenoxy)propyl]piperidine | HCID 19776831 | — |
Reaction Steps
The procedure of Example 36 (a) was repeated except for using di(3-thienyl)methyl chloride and 4-hydroxy-1-[3-(4-methyl-2-nitrophenoxy)propyl]piperidine instead of phenyl-2-thienylmethyl chloride and 4-hydroxy-1-[3-(2-nitrophenoxy)propyl]piperidine to give oily 4-di(3-thienyl)methoxy-1-[3-(4-methyl-2-nitrophenoxy)propyl]piperidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05190959 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-d2ba0fb59a6540898ff32db8fd9dc5ee |
| Source note | uspto-grants-1993_03 |