HCID 19776917, compound → HCID 19776907, compound

HRID 1612869Notes

Reaction equation

HRID 1612869 reaction equation
CN(C)C([S:5][C:6]1[C:13]([O:14][CH3:15])=[CH:12][C:11]([CH3:16])=[CH:10][C:7]=1[CH:8]=[O:9])=O.[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[OH:9][CH2:8][C:7]1[CH:10]=[C:11]([CH3:16])[CH:12]=[C:13]([O:14][CH3:15])[C:6]=1[SH:5]

Participants

3

Reactant 2

HCID 19776917HCID 19776917, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 19776907HCID 19776907, compound

Procedure

59 g (0.23 mol) of the compound from Example 14 are reduced with 11.4 g (0.3 mol) of lithium aluminium hydride analogously to Example 6.

Sources & evidence

ORD record
ord-a8c77cefd0cd42e3b0cdc020348c1735
Source dataset
uspto-grants-1993_03
Patent number
US05190971

Reaction notes

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