HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19776895, compound → HCID 19776913, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19776895 | HCID 19776895 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19776913 | HCID 19776913 | — |
Reaction Steps
31 mg (0.15 mmol) of pyridinium chlorochromate are added to a solution of 35 mg (0.07 mmol) of the compound from Example XV in 4 ml of dichlormethane and the mixture is stirred at room temperature for 2 hours. The reaction solution is applied to silica gel, eluted with dichloromethane and chromatographed on silica gel using petroleum ether/ethyl acetate 1:3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05190971 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-f0dbf35eda1e43a491864bad6d848f3b |
| Source note | uspto-grants-1993_03 |