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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1612875Generated: November 2, 2026

HCID 19776895, compound → HCID 19776913, compound

https://huagongshe.com/reaction/1612875

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 19776895HCID 19776895—
ReactantHCID 178418287HCID 178418287—
SolventDichloromethaneHCID 6344—
ProductHCID 19776913HCID 19776913—

Reaction Steps

31 mg (0.15 mmol) of pyridinium chlorochromate are added to a solution of 35 mg (0.07 mmol) of the compound from Example XV in 4 ml of dichlormethane and the mixture is stirred at room temperature for 2 hours. The reaction solution is applied to silica gel, eluted with dichloromethane and chromatographed on silica gel using petroleum ether/ethyl acetate 1:3.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05190971
Source datasetuspto-grants-1993_03
ORD IDord-f0dbf35eda1e43a491864bad6d848f3b
Source noteuspto-grants-1993_03