HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → Ethyl D-glucoside
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 54493907 | HCID 54493907 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Ethyl D-glucoside | HCID 121667 | — |
Reaction Steps
The ethyl 2,3,4,6-tetra-O-acetyl-glucopyranoside was deacetylated with 1M sodium methoxide (2 ml) in Methanol (80 ml) for 20 hours at room temperature. The mixture was neutralized with Amberlite™ IR-120 (H+ -form) and concentrated in vacuo to give the product in quantitative yield as a hygroscopic solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05191071 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-7281024790d34009b59d906802dbfe5f |
| Source note | uspto-grants-1993_03 |