Cesium fluoride → Allyl Oxalofluoride

HRID 1612931Notes

Reaction equation

HRID 1612931 reaction equation
[CH2:1]([O:4][C:5](=[O:9])[C:6](Cl)=[O:7])[CH:2]=[CH2:3].[F-:10].[Cs+]>>[CH2:1]([O:4][C:5](=[O:9])[C:6]([F:10])=[O:7])[CH:2]=[CH2:3]

Participants

3

Reactant 2

HCID 25953Cesium fluorideHCID 3018516Allyl chlorooxoacetate

Product 1

HCID 14153244Allyl Oxalofluoride

Procedure

By the procedure of the preceding Preparation, allyl oxalochloride (252.5 g, 1.70 mol) and cesium fluoride (284 g, 1.87 mol) were converted to twice distilled title product, b.p. 48°-50° C./35 mm; 124°-126° C. (atmospheric pressure).

Workup

  1. distillationto twice distilled title product, b.p. 48°-50° C./35 mm
  2. custom124°-126° C. (atmospheric pressure)

Sources & evidence

ORD record
ord-85a944180bad405fab9827f31ab725a5
Source dataset
uspto-grants-1993_03
Patent number
US05191077

Reaction notes

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