HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Acetylnaphthalene → 2-Vinylnaphthalene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Acetylnaphthalene | HCID 13663 | — |
| Reactant | HCID 13779418 | HCID 13779418 | — |
| Product | 2-Vinylnaphthalene | HCID 13230 | — |
Reaction Steps
The crude hydrogenated product may therefore be treated to recover the desired methylnaphthyl carbinol in a relatively pure form. This may be effected by distilling the crude hydrogenation product at a pressure sufficiently below atmospheric to give a temperature below that which substantial dehydration of the methylnaphthyl carbinol takes place. Alternatively, it has been found that 2-methylnaphthyl carbinol which is produced can be dehydrated in the presence of 1-acetonaphthalene to yield 2-vinylnaphthalene. The 1-acetonaphthalene remains unreacted.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05191133 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-c4c62e9bf6884c4db74ead8ea0881d26 |
| Source note | uspto-grants-1993_03 |