HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14986289, compound → 4-(3,4-Dimethoxyphenyl)butan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14986289 | HCID 14986289 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-(3,4-Dimethoxyphenyl)butan-1-ol | HCID 12220582 | 93.2% |
Reaction Steps
A mixture of 2.0 g of 4-(3,4-dimethoxyphenyl)-3-butyn-1-ol and 0.2 g of 10% palladium on carbon in 40 mL of ethanol was stirred in a hydrogen atmosphere for 4 hours. After filtration, the filtrate was concentrated under reduced pressure to give 1.9 g of 4-(3,4-dimethoxyphenyl)butan-1-ol as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05191108 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-cad85e73c50b4ee1874332053c84267f |
| Source note | uspto-grants-1993_03 |