Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Nitrogen | HCID 947 | — |
| Reactant | Lauric Acid | HCID 3893 | — |
| Reactant | Pentaerythritol | HCID 8285 | — |
| Product | Pentaerythritol tetralaurate | HCID 12767865 | — |
Reaction Steps
A 1000 ml round bottomed flask was charged with 619.9 g (0.12 mol) PEG 150 pentaerythritol and 96.0 g (0.48 mol) lauric acid. The mass was heated to 100° C. with a N2 sparge, 1.0 g. phosphoric acid and 0.1 g. hypophosphorus acid were charged. The batch was heated to 215° C. while collecting the water of reaction, and maintained until an acid value of 12.4 was reached. The finished material was a white waxy solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05192462 |
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| Source dataset | uspto-grants-1993_03 |
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| ORD ID | ord-a9af03cb409a44ec99f0542d504f6f9a |
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| Source note | uspto-grants-1993_03 |
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