HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl carbazate → HCID 19775376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl carbazate | HCID 80519 | — |
| Reactant | HCID 19775370 | HCID 19775370 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19775376 | HCID 19775376 | 54.3% |
Reaction Steps
In 60 ml of methanol were refluxed 2.00 g (8.1 mmol) of Compound b prepared in Example 2 and 1.10 g (12.2 mmol) of methoxycarbonylhydrazine for 6 hours. The reaction mixture was cooled to obtain 1.32 g (54%) of the titled compound as a colorless crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05192768 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-6749a98a16d9424bbdbc5878a96df070 |
| Source note | uspto-grants-1993_03 |