1-(2-Bromoethyl)-4-methoxybenzene → HCID 19775321, compound

HRID 1613173Notes

Reaction equation

HRID 1613173 reaction equation
[NH2:1][C:2]1([CH2:7][O:8][CH:9]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)[C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[CH2:6][CH2:5][CH2:4][CH2:3]1.[CH3:22][O:23][C:24]1[CH:32]=[CH:31][C:27]([CH2:28][CH2:29]Br)=[CH:26][CH:25]=1>>[C:16]1([CH:9]([C:10]2[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=2)[O:8][CH2:7][C:2]2([NH:1][CH2:29][CH2:28][C:27]3[CH:31]=[CH:32][C:24]([O:23][CH3:22])=[CH:25][CH:26]=3)[CH2:6][CH2:5][CH2:4][CH2:3]2)[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

Participants

3

Reactant 2

HCID 844271-(2-Bromoethyl)-4-methoxybenzeneHCID 19775316HCID 19775316, compound

Product 1

HCID 19775321HCID 19775321, compound

Procedure

The title compound was prepared as described in Example 1 using 1-amino-1-diphenylmethoxymethylcyclopentane (see Preparation 4) and 4-methoxyphenethyl bromide. The title compound was obtained as a pale brown oil which was characterised as a hydrate (0.50 g, 49%).

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-392ac0f8d28648b9bed6aebc6e0f4ad4
Source dataset
uspto-grants-1993_03
Patent number
US05192765

Reaction notes

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