Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | Anthracene | HCID 8418 | — |
| Product | Nsc122884 | HCID 275804 | — |
Reaction Steps
Anthracene (89.0 gm) was combined with methyl acrylate (51.5 gm) and xylenes (500 ml) in a Parr bomb and heated to 210° C. for 12 hours. The solvent was removed on a rotary evaporator and the residue was recrystallized from methanol to provide the product as a white solid (mp=113°-114° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05192762 |
|---|
| Source dataset | uspto-grants-1993_03 |
|---|
| ORD ID | ord-1cbbd07593644d39aef97d991e10ead3 |
|---|
| Source note | uspto-grants-1993_03 |
|---|
