N'-((Dimethylamino)methylene)-N,N-dimethylformohydrazonamide → 4-[2-(2,4-Dichlorophenyl)hexyl]-1,2,4-triazole

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Reaction Steps

A mixture of 10 g (0.04 mole) of 2-(2,4-dichlorophenyl)hexyl amine, 5.7 g (0.04 mole) of N,N-dimethyl formamide azine and 0.5 g of p-toluene sulfonic acid in 100 ml of dry toluene is heated under reflux for 16 hours. The solvent is evaporated to give 15 g of a white solid which can be further purified by recrystallization from benzene to give 7.5 g of pure product.

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