HuagongsheHuagongshe Chemistry Print Report · For research reference only
Borane → 2-(3,4-Dichlorophenoxy)ethan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Borane | HCID 6331 | — |
| Reactant | (3,4-Dichlorophenoxy)acetic acid | HCID 11495 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-(3,4-Dichlorophenoxy)ethan-1-ol | HCID 19108692 | 91% |
Reaction Steps
The title compound was prepared by reduction of 2-(3,4-dichlorophenoxy)acetic acid (Aldrich, 96% pure) with borane in tetrahydrofuran (Aldrich, 1M solution) using the procedure of N. M. Yoon, et al. in J. Org. Chem 38(#16) p. 2786 (1973). The yield was 91% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05192785 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-7b0e61847cba4038b8a679e3b6d599da |
| Source note | uspto-grants-1993_03 |