2-(4-Chlorophenoxy)ethanol → 2-(4-Chlorophenoxy)ethanol sulfamate

HRID 1613366노트

반응식

HRID 1613366 반응식
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[Cl:6][C:7]1[CH:16]=[CH:15][C:10]([O:11][CH2:12][CH2:13][OH:14])=[CH:9][CH:8]=1>>[Cl:6][C:7]1[CH:16]=[CH:15][C:10]([O:11][CH2:12][CH2:13][O:14][S:1](=[O:4])(=[O:3])[NH2:2])=[CH:9][CH:8]=1

참가 물질

3

반응물 2

HCID 159072-(4-Chlorophenoxy)ethanolHCID 24499Chlorosulfamic acid

생성물 1

HCID 191086672-(4-Chlorophenoxy)ethanol sulfamate수율 48%

실험 절차

The title compound was prepared by procedures of Example 22 from sulfamoyl chloride and 2-(4-chlorophenoxy)ethanol in 48% yield. A white solid, mp 117°-119° C. was obtained.

후처리

  1. customA white solid, mp 117°-119° C. was obtained

출처 및 근거

ORD 기록
ord-f6cacc419e4240afab8512b370c06c90
출처 데이터셋
uspto-grants-1993_03
특허 번호
US05192785

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