HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorosulfamic acid → Sulfamic acid 2-(3-methylphenoxy)ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorosulfamic acid | HCID 24499 | — |
| Reactant | Ethanol, 2-(3-methylphenoxy)- | HCID 83611 | — |
| Product | Sulfamic acid 2-(3-methylphenoxy)ethyl ester | HCID 19829505 | 47% |
Reaction Steps
The title compound was prepared by procedures of Example 22 from sulfamoyl chloride and 2-(3-methylphenoxy)ethanol in 47% yield (recrystallizing from the same solvent). A white solid, mp 76°-78° C., was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05192785 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-c991982c83fd40b69953d0dc3ed06e82 |
| Source note | uspto-grants-1993_03 |