Ethanol, 2-(o-tolyloxy)- → 2-(2-Methylphenoxy)ethanol sulfamate

HRID 1613371Notes

Reaction equation

HRID 1613371 reaction equation
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[CH3:6][C:7]1[CH:16]=[CH:15][CH:14]=[CH:13][C:8]=1[O:9][CH2:10][CH2:11][OH:12]>>[CH3:6][C:7]1[CH:16]=[CH:15][CH:14]=[CH:13][C:8]=1[O:9][CH2:10][CH2:11][O:12][S:1](=[O:4])(=[O:3])[NH2:2]

Participants

3

Reactant 2

HCID 22539Ethanol, 2-(o-tolyloxy)-HCID 24499Chlorosulfamic acid

Product 1

HCID 191086612-(2-Methylphenoxy)ethanol sulfamateYield 53%

Procedure

The title compound was prepared by procedures of Example 28 from sulfamoyl chloride and 2-(2-methylphenoxy)ethanol in 53% yield as an off-white solid, mp 81.5°-83° C.

Sources & evidence

ORD record
ord-e3cbad94a0f14be1852f07deb5381e9b
Source dataset
uspto-grants-1993_03
Patent number
US05192785

Reaction notes

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