Chlorosulfamic acid → HCID 19733467, compound

HRID 1613375Notes

Reaction equation

HRID 1613375 reaction equation
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[CH3:6][O:7][C:8]1[CH:9]=[C:10]2[C:15](=[CH:16][CH:17]=1)[CH:14]=[C:13]([CH:18]([CH3:21])[CH2:19][OH:20])[CH:12]=[CH:11]2>>[CH3:6][O:7][C:8]1[CH:9]=[C:10]2[C:15](=[CH:16][CH:17]=1)[CH:14]=[C:13]([CH:18]([CH3:21])[CH2:19][O:20][S:1](=[O:4])(=[O:3])[NH2:2])[CH:12]=[CH:11]2

Participants

3

Reactant 2

HCID 24499Chlorosulfamic acidHCID 3334137414-52-1

Product 1

HCID 19733467HCID 19733467, compoundYield 21%

Procedure

The title compound was prepared by the procedure of Example 28 from sulfamoyl chloride and 2-(6-methoxy-2-naphthyl)propanol as white solid, mp 112°-115° C., in 21% yield.

Sources & evidence

ORD record
ord-91441c52073a4114b461f6c01b362378
Source dataset
uspto-grants-1993_03
Patent number
US05192785

Reaction notes

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