Chlorosulfamic acid → 2-(4-Chlorophenoxy)-2-methylpropanol sulfamate

HRID 1613378Notes

Reaction equation

HRID 1613378 reaction equation
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[Cl:6][C:7]1[CH:18]=[CH:17][C:10]([O:11][C:12]([CH3:16])([CH3:15])[CH2:13][OH:14])=[CH:9][CH:8]=1>>[Cl:6][C:7]1[CH:18]=[CH:17][C:10]([O:11][C:12]([CH3:15])([CH3:16])[CH2:13][O:14][S:1](=[O:4])(=[O:3])[NH2:2])=[CH:9][CH:8]=1

Participants

3

Reactant 2

HCID 24499Chlorosulfamic acidHCID 191086602-(4-Chlorophenoxy)-2-methylpropan-1-ol

Product 1

HCID 197334572-(4-Chlorophenoxy)-2-methylpropanol sulfamateYield 58%

Procedure

The title compound was prepared by procedures of Example 28 from sulfamoyl chloride and 2-(4-chlorophenoxy)-2-methylpropanol to give white solid, mp 76°-79° C., in 58% yield.

Workup

  1. customto give white solid, mp 76°-79° C.

Sources & evidence

ORD record
ord-f1b5fde062be4e26bd3a48dab5ce76b4
Source dataset
uspto-grants-1993_03
Patent number
US05192785

Reaction notes

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