Chlorosulfamic acid → HCID 19108675, compound

HRID 1613380Notes

Reaction equation

[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[Br:6][C:7]1[CH:16]=[CH:15][C:10]([O:11][CH2:12][CH2:13][OH:14])=[CH:9][CH:8]=1>>[Br:6][C:7]1[CH:16]=[CH:15][C:10]([O:11][CH2:12][CH2:13][O:14][S:1](=[O:4])(=[O:3])[NH2:2])=[CH:9][CH:8]=1

Participants

Reactant 2

HCID 24499Chlorosulfamic acid

HCID 991682-(p-Bromophenoxy)ethanol

Product 1

HCID 19108675HCID 19108675, compoundYield 69%

Procedure

The title compound was prepared by the procedures of Example 28 from sulfamoyl chloride and 2-(4-bromophenoxy)ethanol as white solid, mp 134°-137° C., in 69% yield.

Sources & evidence

ORD record: ord-335129901e7c4ba2b18c268f3bfff3c9
Source dataset: uspto-grants-1993_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05192785

Reaction notes

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