HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetonitrile → HCID 10420257, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetonitrile | HCID 8794 | — |
| Reactant | 3-Cyanophenol | HCID 13394 | — |
| Reactant | Chlorosulfonyl isocyanate | HCID 70918 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 10420257 | HCID 10420257 | 85% |
Reaction Steps
Using the procedure described in Example 75, the title compound was prepared in 85% yield from 10.3 g (0.086 mole) of 3-cyanophenol and 8.3 ml (0.086 mole) of chlorosulfonyl isocyanate in 75 ml of toluene as a white solid, mp 101°-104° C. (benzene-acetonitrile).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05192785 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-772164e5d4204b95aa3bef7016928d31 |
| Source note | uspto-grants-1993_03 |