Benzene → HCID 10108748, compound

HRID 1613425Notes

Reaction equation

HRID 1613425 reaction equation
[I:1][C:2]1[CH:3]=[C:4]([OH:8])[CH:5]=[CH:6][CH:7]=1.Cl[S:10]([N:13]=C=O)(=[O:12])=[O:11].C1C=CC=CC=1>C1(C)C=CC=CC=1>[I:1][C:2]1[CH:3]=[C:4]([O:8][S:10](=[O:12])(=[O:11])[NH2:13])[CH:5]=[CH:6][CH:7]=1

Participants

5

Reactant 3

HCID 241BenzeneHCID 122723-IodophenolHCID 70918Chlorosulfonyl isocyanate

Product 1

HCID 10108748HCID 10108748, compoundYield 78%

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

This compound was prepared using the procedure of Example 75 from 27.8 g (0.126 mole) of 3-iodophenol and 11.7 ml (0.135 mole) of chlorosulfonyl isocyanate in 100 ml of toluene to obtain 29.4 g (78%) of the title compound as white flakes, mp 106°-108° C. (benzene).

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-3a6638eb090347d4b01224fe8c4f1fc8
Source dataset
uspto-grants-1993_03
Patent number
US05192785

Reaction notes

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