HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyanophenol → HCID 44459430, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyanophenol | HCID 13019 | — |
| Reactant | Chlorosulfonyl isocyanate | HCID 70918 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 44459430 | HCID 44459430 | 51% |
Reaction Steps
This compound was prepared by the procedure of Example 75 from a solution of 11.9 g (0.10 mole) of 4-cyanophenol (Aldrich Chemical Co.) and 9.1 ml (0.105 mole) of chlorosulfonyl isocyanate in 75 ml of toluene. The solid product was recrystallized from benzene-acetonitrile to give 10.1 g (51%) of white solid, mp 154°-156° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05192785 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-c0e710770ef148dbb1e64c0eee3c70df |
| Source note | uspto-grants-1993_03 |