HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene methanol → (4-Nitrophenyl)hydrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene methanol | HCID 21867641 | — |
| Reactant | HCID 135981640 | HCID 135981640 | — |
| Solvent | HCID 11627212 | HCID 11627212 | — |
| Product | (4-Nitrophenyl)hydrazine | HCID 3310889 | — |
Reaction Steps
2-(3,7,11,15-tetramethyl-2-hexadecenyl)-3-methyl-4-[(4-nitrophenyl)azo]-1-naphthol, TLC, silica gel 60 (Merck), mobile solvent: toluol/methanol=50:1; Rf =0.22, from 4-nitrophenylhydrazine, Transmission spectra at an acid or alkaline pH in o-nitrophenyloctyl ether yield λmax values of 455 or 637 nm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05194389 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-39250f26f8644a84ba980e52d0414256 |
| Source note | uspto-grants-1993_03 |