Chlorosulfamic acid → HCID 19108682, compound

HRID 1613749Notes

Reaction equation

HRID 1613749 reaction equation
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[CH3:6][O:7][C:8]1[CH:17]=[CH:16][C:11]([O:12][CH2:13][CH2:14][OH:15])=[CH:10][CH:9]=1>>[S:1]([O:15][CH2:14][CH2:13][O:12][C:11]1[CH:16]=[CH:17][C:8]([O:7][CH3:6])=[CH:9][CH:10]=1)(=[O:4])(=[O:3])[NH2:2]

Participants

3

Reactant 2

HCID 24499Chlorosulfamic acidHCID 2200792-(4-Methoxyphenoxy)ethanol

Product 1

HCID 19108682HCID 19108682, compoundYield 54%

Procedure

The title compound was prepared by procedures of Example 33 from sulfamoyl chloride and 2-(4-methoxyphenoxy)ethanol in 54% yield as an off-white solid, mp 84°-87° C.

Sources & evidence

ORD record
ord-cacb9ad89cfd4090a7e13ade92dea77f
Source dataset
uspto-grants-1993_03
Patent number
US05194446

Reaction notes

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