Chlorosulfamic acid → HCID 86746621, compound

HRID 1613753Notes

Reaction equation

HRID 1613753 reaction equation
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[CH3:6][CH:7]([CH3:19])[CH2:8][C:9]1[CH:14]=[CH:13][C:12]([CH:15]([CH3:18])[CH2:16][OH:17])=[CH:11][CH:10]=1>>[CH3:6][CH:7]([CH3:19])[CH2:8][C:9]1[CH:10]=[CH:11][C:12]([CH:15]([CH3:18])[CH2:16][OH:17])=[CH:13][CH:14]=1.[S:1](=[O:4])(=[O:17])([O-:3])[NH2:2]

Participants

3

Reactant 2

HCID 24499Chlorosulfamic acidHCID 595160β-Methyl-4-(2-methylpropyl)benzeneethanol

Product 1

HCID 86746621HCID 86746621, compound

Procedure

The title compound was prepared by procedures of Example 33 from sulfamoyl chloride and 2-[4-(2-methylpropyl)phenyl]-propan-1-ol. The oil obtained was further purified as in Example 38 to give the title compound as a white solid, mp 61°-63° C. in 45% yield.

Workup

  1. customThe oil obtained
  2. customwas further purified as in Example 38

Sources & evidence

ORD record
ord-1766ce101fd442ebac79c52f6cf23323
Source dataset
uspto-grants-1993_03
Patent number
US05194446

Reaction notes

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