HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Phenoxy-1-propanol → 2-Phenoxypropanol sulfamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Phenoxy-1-propanol | HCID 20129 | — |
| Reactant | Chlorosulfamic acid | HCID 24499 | — |
| Product | 2-Phenoxypropanol sulfamate | HCID 19108685 | — |
Reaction Steps
The title compound was prepared by procedures of Example 33 from sulfamoyl chloride and 2-phenoxypropanol. The oil obtained was further purified as in Example 38 by chromatography and recrystallization to give the title compound as colorless, viscous oil in 35% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05194446 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-26c5d0112baf40db9bcfeabdc0e5ec20 |
| Source note | uspto-grants-1993_03 |