Chlorosulfamic acid → HCID 19108702, compound

HRID 1613758Notes

Reaction equation

HRID 1613758 reaction equation
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[Cl:6][C:7]1[CH:8]=[C:9]([CH:14]=[CH:15][CH:16]=1)[O:10][CH2:11][CH2:12][OH:13]>>[S:1]([O:13][CH2:12][CH2:11][O:10][C:9]1[CH:14]=[CH:15][CH:16]=[C:7]([Cl:6])[CH:8]=1)(=[O:4])(=[O:3])[NH2:2]

Participants

3

Reactant 2

HCID 24499Chlorosulfamic acidHCID 802702-(3-Chlorophenoxy)ethanol

Product 1

HCID 19108702HCID 19108702, compoundYield 44%

Procedure

The title compound was prepared by procedures of Example 33 from sulfamoyl chloride and 2-(3-chlorophenoxy)ethanol. The oil obtained was further purified by chromatography and recrystallization as in Example 38 to give white solid, mp 66°-69° C., in 44% yield.

Workup

  1. customThe oil obtained
  2. customwas further purified by chromatography and recrystallization as in Example 38
  3. customto give white solid, mp 66°-69° C.

Sources & evidence

ORD record
ord-47eff2fab8b14f4eb2fa38c2eca0c547
Source dataset
uspto-grants-1993_03
Patent number
US05194446

Reaction notes

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