HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → Benzyl sulfamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | Chlorosulfamic acid | HCID 24499 | — |
| Product | Benzyl sulfamate | HCID 9990000 | 38% |
Reaction Steps
The title compound was prepared by the procedures of Example 33 from sulfamoyl chloride and benzyl alcohol being careful to use reduced pressure at about 35° C. to remove solvents in order to avoid violent decomposition observed in another trial at higher temperature. A white solid, mp 75°-78° C., was obtained in 38% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05194446 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-98549ebc5a644c70a0efd1f1ff437bbc |
| Source note | uspto-grants-1993_03 |