HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Iodophenol → HCID 44459431, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Iodophenol | HCID 10894 | — |
| Reactant | Chlorosulfonyl isocyanate | HCID 70918 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 44459431 | HCID 44459431 | 80% |
Reaction Steps
This compound was prepared according to the procedure of Example 56. A mixture of 22.0 g (0.1 mole) of 4-iodophenol (Aldrich) and 9.1 ml (14.8 g, 0.105 mole) of chlorosulfonyl isocyanate in 100 ml of toluene gave 23.8 g (80%) of the title compound as a white solid, mp 146°-147° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05194446 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-99cbbb5267f643948d6f2140b684d093 |
| Source note | uspto-grants-1993_03 |