Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hexane | HCID 8058 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Lithium, 1H-inden-1-yl- | HCID 11116044 | — |
Reaction Steps
A 250 mL Schlenk flask is charged with diethyl ether, 100 mL, then chilled to -20° C. To the chilled solvent is added n-butyllithium, 5.4 mL of a 2.79 M in hexane (15 mmole). To the magnetically stirred mixture is added nitrogen degassed indene, 1.92 mL (16.5 mmole). The mixture is stirred overnight at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05194532 |
|---|
| Source dataset | uspto-grants-1993_03 |
|---|
| ORD ID | ord-2d4743b7fbd648b598c78739e548a985 |
|---|
| Source note | uspto-grants-1993_03 |
|---|
