Formic Acid → Formamide, N-(2-(7-methoxy-1-naphthalenyl)ethyl)-

HRID 1613909Notes

Reaction equation

HRID 1613909 reaction equation
[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([CH:7]=[CH:8][CH:9]=[C:10]2[CH2:13][CH2:14][NH2:15])=[CH:5][CH:4]=1.[CH:16](O)=[O:17]>>[CH3:1][O:2][C:3]1[CH:12]=[C:11]2[C:6]([CH:7]=[CH:8][CH:9]=[C:10]2[CH2:13][CH2:14][NH:15][CH:16]=[O:17])=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 284Formic AcidHCID 110526677-Methoxy-1-naphthaleneethanamine

Product 1

HCID 3071657Formamide, N-(2-(7-methoxy-1-naphthalenyl)ethyl)-

Conditions

Temperature
120 °C

Procedure

0.01 mol of 2-(7-methoxynaphth-1-yl)ethylamine and 0.02 mol of formic acid are placed in a porcelain crucible, and heated at 120° C. until a dry residue is obtained. This is recrystallized.

Workup

  1. customis obtained
  2. customThis is recrystallized

Sources & evidence

ORD record
ord-a96abfa900dc40f3b809a57c4ac73f2d
Source dataset
uspto-grants-1993_03
Patent number
US05194614

Reaction notes

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