HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-furyl)-1,4-pentanedione → HCID 19774594, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-furyl)-1,4-pentanedione | HCID 2741848 | — |
| Reactant | Methylenechloride Hexane | HCID 21226440 | — |
| Product | HCID 19774594 | HCID 19774594 | 70% |
Reaction Steps
16.6 g (100 mmol}of 1-(2-furyl)-1,4-pentanedione were reacted analogously to Example 8. Column chromatography with hexane/methylene chloride (7:1) as the mobile phase gave 13.7 g (70 %) of the indene 13. For the NMR data, see Table 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05194619 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-7c57edfa18c94ebe8e22e983c1a6cc1e |
| Source note | uspto-grants-1993_03 |