HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → 3-Hydroxypropyl Dimethyl Nonyl Ammonium Iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 1-Iodononane | HCID 20275 | — |
| Reactant | Propanol, (dimethylamino)- | HCID 116739 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 3-Hydroxypropyl Dimethyl Nonyl Ammonium Iodide | HCID 19774828 | 77% |
Reaction Steps
Employing the procedure of EXAMPLE II, 20.0 g of nonyl iodide was reacted with 14.3 ml of N,N-dimethylaminopropanol in 50 ml of acetonitrile to provide a crude product which was slurried with ether to give 27 g (77%) of an amber oil which solidified on standing. Proton NMR confirmed the desired structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05194667 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-d2060ecb37a04a32893fe286ab4cde1e |
| Source note | uspto-grants-1993_03 |