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HRID 1614250作成日：2026年10月25日

Ethylamine hydrochloride → 5-Acetylamino-2-ethylamino-tetraline-hydrochloride

https://huagongshe.com/reaction/1614250

反応式

関与物質

役割名称HCID仕込み量
反応物Ethylamine hydrochlorideHCID 11198—
反応物5-Acetylamino-2-tetraloneHCID 14836456—
生成物5-Acetylamino-2-ethylamino-tetraline-hydrochlorideHCID 19773324—

反応手順

Starting from 2.03 g (0.01 mol) of 5-acetylamino-2-tetralone and 2.45 g (0.03 mol) of ethylaminehydrochloride the title compound is obtained analogously to Example 4.1.11 in a yield of 1.2 g (44.6% of theory) and with a melting point of 351° C. which does not change after recrystallisation from methanol/ether.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05196454
出典データセットuspto-grants-1993_03
ORD IDord-a8560640f4b240b8941e76191c941a04
出典メモuspto-grants-1993_03