HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2Z)-3-phenylprop-2-en-1-amine hydrochloride → 5-Acetylamino-2-(cis-cinnamylamino)-tetralinehydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2Z)-3-phenylprop-2-en-1-amine hydrochloride | HCID 12219098 | — |
| Reactant | 5-Acetylamino-2-tetralone | HCID 14836456 | — |
| Product | 5-Acetylamino-2-(cis-cinnamylamino)-tetralinehydrochloride | HCID 70057793 | — |
Reaction Steps
Starting from 1.02 g (0.005 mol) of 5-acetylamino-2-tetralone and 1.7 g (0.01 mol) of cis-cinnamyl-aminehydrochloride the title compound is obtained analogously to Example 4.1.11 in a yield of 1.35 g (76.5% of theory) and with a melting point of 246° C., which does not change after recrystallisation from methanol/ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05196454 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-70832d8e62904136885f3a92567084f2 |
| Source note | uspto-grants-1993_03 |