HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodopropane → HCID 19773413, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodopropane | HCID 33643 | — |
| Reactant | HCID 14836523 | HCID 14836523 | — |
| Product | HCID 19773413 | HCID 19773413 | — |
Reaction Steps
Starting from 2.88 g (0.010 mol) of 5-acetylamino-2-di-n-propylamino-tetraline (Example 4.3.4) and 2.04 g (0.012 mol) of n-propyliodide, the title compound is obtained analogously to Example 4.7.1 in the form of a non-crystallising gum in a yield of 2.70 g (89.4% of theory) and with an Rf value of 0.67 (solvent mixture as specified in 4.7.1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05196454 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-b1921b91e86a4f798bf4231261e30b21 |
| Source note | uspto-grants-1993_03 |