HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → N-(2-benzoyloxyethyl)pyridinium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 2-Bromoethyl Benzoate | HCID 523090 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | N-(2-benzoyloxyethyl)pyridinium bromide | HCID 19762119 | — |
Reaction Steps
A solution of 50.0 grams (0.218 mol) of 2-bromoethyl benzoate, 17.27 grams (0.218 mol) of pyridine and 135 milliters of acetonitrile was heated at reflux for 17.75 hours and cooled. Solid crystallized and was collected, washed with acetonitrile, then with ether and dried. The yield of product was 48.5 grams (72.19% of theory); mp=162°-164° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05196539 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-f6b9a5e6dde7443fb18861aa01558bb6 |
| Source note | uspto-grants-1993_03 |