HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Carbonate → 4-(Methoxymethyl)-1,3-dioxolan-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Carbonate | HCID 7766 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 3-Methoxy-1,2-propanediol | HCID 92822 | — |
| Product | 4-(Methoxymethyl)-1,3-dioxolan-2-one | HCID 4384485 | — |
Reaction Steps
A mixture of 14 g (0.132 mol) of 3-methoxypropane-1,2-diol (S)and 31.16 g (0.264 mol) of diethyl carbonate in the presence of 0.108 g of 50% sodium hydride is heated until distillation of the alcohol formed. After completion of the reaction, the aimed product is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05196543 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-2538b0302d7d4bf796b8448851806dfb |
| Source note | uspto-grants-1993_03 |