HCID 19745106, compound → HCID 86746662, compound

HRID 1614373Notes

Reaction equation

HRID 1614373 reaction equation
[Br-].[CH:2]1([C:8]2([CH2:13][CH2:14][P+:15]([C:28]3[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=3)([C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=3)[C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)[O:12][CH2:11][CH2:10][O:9]2)[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3]1.[CH:34]1(C2(CC[Br:47])OCCO2)CCCCC1>>[Br-:47].[C:7]1([CH2:2][C:8]2([CH2:13][CH2:14][P+:15]([C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)([C:22]3[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=3)[C:28]3[CH:29]=[CH:30][CH:31]=[CH:32][CH:33]=3)[O:9][CH2:10][CH2:11][O:12]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:34]=1

Participants

3

Reactant 2

HCID 19745106HCID 19745106, compoundHCID 19745116HCID 19745116, compound

Product 1

HCID 86746662HCID 86746662, compound

Procedure

[2-(2-cyclohexyl-1,3-dioxolane-2-yl)ethyl]triphenylphosphonium bromide from 2-cyclohexyl-2-(2-bromoethyl)-1,3-dioxolane (ex. 27): Liq., IR (microcell) ν cm-1 : 2920-2850, 1440-1110;

Sources & evidence

ORD record
ord-1c271a07a353473794973c8acf6d9605
Source dataset
uspto-grants-1993_03
Patent number
US05196543

Reaction notes

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