Hydrate lead acetate → Lead(2+);bis(1-methoxyethanolate)

HRID 1614504Notes

Reaction equation

HRID 1614504 reaction equation
O.[C:2]([O-:5])(=[O:4])[CH3:3].[Pb+2:6].[C:7]([O-:10])(=[O:9])[CH3:8]>COC(O)C>[CH3:7][O:4][CH:2]([CH3:3])[O-:5].[Pb+2:6].[CH3:2][O:9][CH:7]([CH3:8])[O-:10]

Participants

3

Reactant 1

HCID 86584228Hydrate lead acetate

Product 1

HCID 131717835Lead(2+);bis(1-methoxyethanolate)

Reagents, catalysts & solvents 1

HCID 30156371-MethoxyethanolSolvent

Procedure

For the multicomponent PZT and PLZT sol-gel thin films to be described in Examples 8 through 14, stock alkoxide solutions were prepared. A lead methoxyethoxide stock solution was prepared by dissolving 37.9 grams of lead acetate hydrate in 300 ml of methoxyethanol at 80° C. The solution was distilled at 110° C. to remove the water and acetate. This lead methoxyethoxide stock solution was analyzed by ICP (inductively coupled plasma) to have a Pb concentration of 87.8 grams/liter (0.422 M).

Workup

  1. customwere prepared
  2. distillationThe solution was distilled at 110° C.
  3. customto remove the water and acetate

Sources & evidence

ORD record
ord-45ab051d9ed3491a8b2f479c2df3065e
Source dataset
uspto-grants-1993_03
Patent number
US05198269

Reaction notes

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