HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → Methanone, [2-(bromomethyl)phenyl]phenyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 2-Methylbenzophenone | HCID 67230 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | Methanone, [2-(bromomethyl)phenyl]phenyl- | HCID 11778133 | — |
Reaction Steps
A mixture of 2-methylbenzophenone (9.8 g), N-bromosuccinimide (8.9 g), benzoyl peroxide (0.5 g) and carbon tetrachloride (150 ml) was refluxed for 1 hour with light irradiation. The mixture was cooled, and then filtered to remove insoluble substances. The filtrate was concentrated to afford quantitatively the above-titled compound as an oily susbstance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05198462 |
| Source dataset | uspto-grants-1993_03 |
| ORD ID | ord-45c80e9646024cb9882f47db98e06195 |
| Source note | uspto-grants-1993_03 |